Synthesis and properties of γ-Ga2O3–Al2O3 solid solutions View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-10

AUTHORS

T. N. Afonasenko, N. N. Leont’eva, V. P. Talzi, N. S. Smirnova, G. G. Savel’eva, A. V. Shilova, P. G. Tsyrul’nikov

ABSTRACT

The textural and structural properties of mixed oxides Ga2O3–Al2O3, obtained via impregnating γ-Al2O3 with a solution of Ga(NO3)3 and subsequent heat treatment, are studied. According to the results from X-ray powder diffraction, gallium ions are incorporated into the structure of aluminum oxide to form a solid solution of spinel-type γ-Ga2O3–Al2O3 up to a Ga2O3 content of 50 wt % of the total weight of the sample, accompanied by a reduction in the specific surface area, volume, and average pore diameter. It is concluded that when the Ga2O3 content exceeds 50 wt %, the β-Ga2O3 phase is observed along with γ-Ga2O3–Al2O3 solid solution. 71Ga and 27Al NMR spectroscopy shows that gallium replaces aluminum atoms from the tetrahedral position to the octahedral coordination in the structure of γ-Ga2O3–Al2O3. More... »

PAGES

1939-1945

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URI

http://scigraph.springernature.com/pub.10.1134/s003602441710003x

DOI

http://dx.doi.org/10.1134/s003602441710003x

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https://app.dimensions.ai/details/publication/pub.1091834670


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