Monolithic capillary columns based on pentaerythritol tetraacrylate for peptide analysis View Full Text


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Article Info

DATE

2015-09

AUTHORS

E. V. Kucherenko, D. M. Melnik, A. A. Korolev, A. Yu. Kanateva, A. V. Pirogov, A. A. Kurganov

ABSTRACT

Monolythic medium-polar capillary columns based on pentaerythritol tetraacrylate were optimized for separation of peptides. The synthesis temperature and time, the fraction of monomer in the initial polymerization mixture, and the nature of alcohol contained in the complex porogen were chosen as optimization parameters. The highest efficiency was attained for columns obtained with 33 and 34% monomer at a polymerization time of 75 min and a temperature of 75°C. The columns with the optimum structure were effective in separation of a model mixture of five peptides. The sensitivity of the method was 200 ng of peptide per column. More... »

PAGES

1688-1692

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036024415090198

DOI

http://dx.doi.org/10.1134/s0036024415090198

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1003927577


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