Mössbauer Characterization of Electronic States and Local Surroundings of 57Fe and 119Sn in Ca-Substituted Lutetium Orthoferrites Lu1 – xCaxFe0.997Sn0.003O3 View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-12

AUTHORS

E. M. Mezhuev, M. I. Afanasov, D. S. Larionov, M. V. Korolenko, P. B. Fabrichnyi

ABSTRACT

The electronic state and local surrounding of both iron ions and tin dopant ions in Lu1 – xCaxFe0.997Sn0.003O3 (x = 0.003; 0.1; 0.2) compounds were studied by 57Fe and 119Sn Mössbauer spectroscopy. The analysis of 57Fe spectra showed that in the Lu0.8Ca0.2Fe0.997Sn0.003O3 sample, obtained by air annealing, the charge deficit created by the substitution of Lu3+ by Ca2+ was compensated by the partial transition of Fe3+ to the +5 oxidation state. With a further increase in the value of x (in the Lu0.8Ca0.2Fe0.997Sn0.003O3 compound) a mixed compensation mechanism appeared, including the formation of oxygen vacancies VO in addition to Fe5+ ions. Annealing the sample with x = 0.1 in H2 at 400°C led to the reduction of Fe5+ to Fe3+ and, accordingly, to the pure vacancy mechanism of the Ca2+ charge deficit compensation. The analysis of 119Sn spectra showed that the substitution of Lu3+ by Са2+ in the Lu0.8Ca0.2Fe0.997Sn0.003O3 structure led to the increase in the value of the magnetic field H, probed by some Sn4+ ions, as compared to the value of H> observed in the case of Lu0.997Ca0.003Fe0.997Sn0.003O3. This change can be explained by a local increase in the angle of the indirect exchange interaction in the chain Fe3+–О2––Sn4+, reflecting the presence of Ca2+ cation, larger than that of Lu3+, in the vicinity of Sn4+ ion. More... »

PAGES

1610-1616

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s003602361812015x

DOI

http://dx.doi.org/10.1134/s003602361812015x

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