Synthesis, Crystal, and Molecular Structure of bis(Thiosemicarbazide)Nickel(II) 1,5-Naphthalene Disulfonate Dihydrate Complex [Ni(Tsc)2](1,5-Nds) · 2H2O View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-09

AUTHORS

V. S. Sergienko, T. V. Koksharova, M. D. Surazhskaya, T. S. Skakun

ABSTRACT

Complex [Ni(Tsc)2](1.5-Nds) · 2H2O (I), where Tsc = thiosemicarbazide, NH2NHC(=S)NH2; 1,5-Nds2– is double deprotonated anion of 1,5-naphthalene disulfonic acid CH10H6(SO3)22− was synthesized, characterized by IR spectroscopy, and studied by thermogravimetry and X-ray diffraction. Crystal I is built of complex cations [Ni(Tsc)2]2+, anions (Nds)2–, and crystallization water molecules. The Ni atom is coordinated along the vertices of the trans-square by two sulfur atoms and two nitrogen atoms of two bidentate chelating ligands Tsc. The structural units of crystal I are joined by a branched network of N–H···O and O–H···O hydrogen bonds with the participation of donors, namely, the hydrogen atoms of two NH2 groups and the NH group of complex cation [Cu(Tsc)]2+ and the H atoms of water molecules, and acceptors, namely, oxygen atoms of the sulfate group of anion 1,5-Nds2– and solvate water molecules. More... »

PAGES

1171-1177

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023618090176

DOI

http://dx.doi.org/10.1134/s0036023618090176

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1107279741


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