Effect of the Synthesis Conditions on the Crystal, Local, and Electronic Structures of Ce2x4+Ce2-2x3+M2O7 + x (M = Zr, Hf) View Full Text


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Article Info

DATE

2018-04-23

AUTHORS

V. V. Popov, A. P. Menushenkov, R. M. Khubbutdinov, A. A. Yastrebtsev, A. S. Sharapov, Ya. V. Zubavichus, R. D. Svetogorov, A. L. Trigub, N. A. Tsarenko, L. A. Arzhatkina, V. V. Kurilkin

ABSTRACT

The effect of synthesis conditions (type of cations, annealing temperature, reductive or oxidative atmosphere) on the chemical composition and structure of compounds formed in the MO2–CeO2/Ce2O3 systems (M = Zr, Hf) was studied by X-ray diffraction, X-ray absorption spectroscopy, Raman spectroscopy, and thermogravimetric analysis. The isothermal annealing of the precursors at temperatures below 1000°C in air gives Ce0.5M0.5O2 powders with fluorite type cubic structure (space group Fm3̅m). High-temperature annealing above 1000°C gives rise to additional tetragonal (space group P42/nmc) (for zirconates) or monoclinic (space group P21/a) (for hafnates) phases. The annealing in a hydrogen atmosphere affords the compounds Ce2x4+Ce2-2x3+M2O7 + x with an intermediate oxidation state of cerium and the x value depending on both the reduction conditions and the pre-annealing parameters. Vacuum annealing at 1400°C considerably decreases the content of Ce(IV) in the samples and affords a pyrochlore structure (space group Fd3̅m) with predominating Ce(III) cations. More... »

PAGES

503-511

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023618040150

DOI

http://dx.doi.org/10.1134/s0036023618040150

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