Bis(Thiosemicarbazide)Copper(II) 1,5-Naphthalenedisulfonate Complex [Cu(Тsc)2](1,5-Nds): Synthesis and Crystal and Molecular Structures View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-01

AUTHORS

V. S. Sergienko, T. V. Koksharova, M. D. Surazhskaya, T. S. Skakun, Yu. N. Mikhailov

ABSTRACT

The synthesis, analysis, and IR spectroscopic, thermogravimetric, and X-ray diffraction study of [Cu(Тsc)2](Nds) (I), where Тsc is thiosemicarbazide NH2NHС(=S)NH2, and 1,5-Nds2– is the doubly deprotonated 1,5-naphthalenedisulfoacid anion C10H6(SO3)22–, have been performed. Crystal structure units in complex I are [Cu(Тsc)2]2+ centrosymmetric complex cations and (Nds)2– anions (including those in inversion centers). The copper atom is coordinated to the vertices of a square via the two sulfur and two nitrogen atoms of the two bidentate-chelate (S,N) ligands Тsc. Crystal structure units in complex I are linked together by a branched network of weak nonlinear N–Н···О hydrogen bonds with participation of donors (all the five independent hydrogen atoms of the two NH2 groups and NH group of the [Cu(Tsc)]2+ complex cation) and acceptors (all the three independent oxygen atoms of the sulfato group of the 1,5-Nds2– anion). More... »

PAGES

22-27

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023618010138

DOI

http://dx.doi.org/10.1134/s0036023618010138

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1101382031


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