Electrochemical synthesis and structure of 2-amino-1-ethylbenzimidazole adducts of copper, cobalt, and zinc chelates in the N,N,S ligand environment View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-08

AUTHORS

D. A. Garnovskii, G. G. Aleksandrov, N. I. Makarova, S. I. Levchenkov, V. G. Vlasenko, Ya. V. Zubavichus, A. I. Uraev, A. S. Burlov

ABSTRACT

2-Amino-1-ethylbenzimidazole (L1) adducts with copper(II), cobalt(II), and zinc(II) chelates of N,N,S tridentate tosylamino-functionalized mercaptopyrazole-containing Schiff base (H2L), resulting from condensation of 2-tosylaminoaniline with 1-phenyl-3-methyl-4-formylpyrazole-5-thiol, with the general formula [ML · L1] were obtained by electrochemical method. The structure and composition of the complexes were confirmed by the data of C, H, N elemental analysis, IR and 1H NMR spectroscopy, and magnetochemical and X-ray spectral measurements. The mononuclear structure of the copper(II) adduct with coordination bond located on the pyridine type endocyclic nitrogen atom of 2-amino-1-ethylbenzimidazole was proved by X-ray diffraction. More... »

PAGES

1077-1084

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023617080071

DOI

http://dx.doi.org/10.1134/s0036023617080071

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1091381863


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