Neutron diffraction study of dehydrogenation of titanium carbohydrides TiCxHy View Full Text


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Article Info

DATE

2017-04-29

AUTHORS

I. Khidirov

ABSTRACT

The possibility of the synthesis of hydrogen-nonstoichiometric cubic titanium carbide ТiСх of high purity from powdery nonstoichiometric cubic titanium carbohydride ТiСхHy or nonstoichiometric titanium carbide with admixture hydrogen by annealing in a continuously maintained vacuum of no worse than 1.33 × 10–3 Pa at temperatures of 600–750°C for several hours has been shown. Similar annealing at higher temperatures (T ≥ 800°C) does not lead to the complete removal of hydrogen from a sample due to intensive sintering. In this case, it seems that pores between sintered particles are hydrogen traps, and the release of hydrogen through the surface of sintered particles is hindered. More... »

PAGES

498-502

References to SciGraph publications

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URI

http://scigraph.springernature.com/pub.10.1134/s0036023617040088

DOI

http://dx.doi.org/10.1134/s0036023617040088

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1085079700


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