Products of complexation in the Cu(CH3CОО)2–2-(7-bromo-2-oxo-5-phenyl-3H-1,4-benzodiazepin-1-yl)acetohydrazide–salicylaldehyde–isopropanol system View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2017-02

AUTHORS

A. V. Pulya, I. I. Seifullina, L. S. Skorokhod, N. N. Efimov, E. A. Ugolkova, V. G. Vlasenko, S. I. Levchenkov, A. L. Trigub, Ya. V. Zubavichus, V. V. Minin

ABSTRACT

Copper(II) complexes isolated from the Cu(CH3COO)2–2-(7-bromo-2-oxo-5-phenyl-3H-1,4-benzodiazepin-1-yl)acetohydrazide (Hydr)–salicylaldehyde (HSal)–isopropanol system [Cu2(HydrSal)2(μ-CH3COO)] (I), [Cu(HydrSal)2] (II) (HydrSal (hydrazone)is the condensation product of hydrazide and salicylaldehide) are synthesized and investigated. The complexes are characterized by elemental analysis, electrical conductivity measurements, and IR spectroscopy. The composition and structure of the Cu2+ coordination core are determined by ESR spectroscopy (I), magnetic susceptibility measurements and extended X-ray absorption fine structure (EXAFS) spectroscopy (II). More... »

PAGES

191-196

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023617020139

DOI

http://dx.doi.org/10.1134/s0036023617020139

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1083869999


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