Effect of the introduction procedure and concentration of yttrium cations on the crystal structure of (1–x)ZrO2 · xY2O3 powders View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-11-15

AUTHORS

V. V. Popov, A. A. Yastrebtsev, S. A. Korovin, N. A. Tsarenko, L. A. Arzhatkina

ABSTRACT

An integrated study of the crystal and local structures of complex oxides (1–x)ZrO2 · xY2O3 (x = 0.005–0.18, YSZ), precipitated from solutions of metal salts and annealed in air, was carried out. For the use of deposition from solutions, reverse co-precipitation was found to be the method of choice for introducing yttrium cations into YSZ, ensuring the maximum stabilization effect of high-temperature phases. An increase in the yttrium content induces polymorphic transformations, monoclinic phase (P21/a) → tetragonal phase (P42/nmc) (for x = 0.02) → cubic phase (Fm3¯\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$\bar 3$$\end{document}m) (for x = 0.08), in the samples prepared at temperatures of ≤1000°C. A Raman study of the local structure of YSZ powders confirmed the formation of a single-phase tetragonal structure for the 2YSZ and 3YSZ samples and identified trace amounts of the tetragonal phase for the 8YSZ and 18YSZ samples with the cubic structure. More... »

PAGES

1378-1386

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023616110164

DOI

http://dx.doi.org/10.1134/s0036023616110164

DIMENSIONS

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