cis- and trans-planar four-coordinated palladium(II) azo-5-pyrazolone (thione) complexes with N2O2- and N2S2-ligand environment: Synthesis and structure View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2015-12

AUTHORS

A. S. Burlov, A. I. Uraev, K. A. Lysenko, I. S. Vasil’chenko, S. A. Mashchenko, E. V. Korshunova, D. A. Garnovskii, E. D. Garnovskaya, G. S. Borodkin

ABSTRACT

Three novel palladium(II) azo complexes (I–III), whose compositions and structures were established from C, H, N, S elemental analysis and IR and 1H NMR spectroscopy, were synthesized by boiling palladium(II) acetate and some pyrazolazo derivatives, namely, 2-iso-propyl(phenyl)-3-methyl-4-[(4-meth-ylphenyl)diazenyl]-1H-pyrazol-5-one and 1-iso-propyl-3-methyl-4-[(4-methylphenyl)diazenyl]-1H-pyrazol-5-thione (HL(a–c)) in an acetone/methanol (1: 1) mixture. X-ray diffraction analysis was performed for complexes I and III. Complex I with an N2O2-ligand environment was established to have a trans-planar configuration for the PdN2O2 chelate ring, while the formation of the cis-planar structure by the PdN2S2 chelate ring was typical for complex III. More... »

PAGES

1481-1486

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023615120062

DOI

http://dx.doi.org/10.1134/s0036023615120062

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1053394526


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