Preparation and crystal structure of [Ru2(μ-Cl)3(P(CH2OH)3)6]Cl View Full Text


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Article Info

DATE

2015-07

AUTHORS

A. V. Anyushin, P. A. Abramov, N. B. Kompankov, M. N. Sokolov

ABSTRACT

A new water-soluble phosphine Ru complex, [Ru2(μ-Cl)3(P(CH2OH)3)6]Cl, has been prepared from [Ru(PPh3)3Cl2] and P(CH2OH)3 in methanol. The complex was characterized by X-ray analysis. The crystal system is triclinic, space group , a = 9.3659(1) Å, b = 13.0976(2) Å, c = 16.791(3) Å, α = 105.620(5)°, β = 91.114(6)°, γ = 110.193(3)°, V = 1847.3(5) Å3, Z = 2. It contains [Ru2(μ-Cl)3(P(CH2OH)3)6]+ and Cl− ions, bound together by hydrogen bonds. Ru has octahedral coordination, with Ru-Cl and Ru-P bond lengths of 2.4815(17)–2.5034(15) and 2.2738(18)–2.2772(18) Å, respectively. The RuïRu distance is nonbonding, 3.350(2) Å, which is atypical of Ru(II) complexes. More... »

PAGES

871-874

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http://scigraph.springernature.com/pub.10.1134/s0036023615070025

DOI

http://dx.doi.org/10.1134/s0036023615070025

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