New fluorochromatouranylates of alkali metals: Synthesis and structure View Full Text


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Article Info

DATE

2014-08

AUTHORS

V. N. Serezhkin, E. V. Peresypkina, S. A. Novikov, A. V. Virovets, L. B. Serezhkina

ABSTRACT

Four new fluorochromatouranylates, namely, K[UO2(CrO4)F] · 1.5H2O (I), Rb[UO2(CrO4)F] · 1.5H2O (II), Rb[UO2(CrO4)F] · 0.5H2O (III), and Cs[UO2(CrO4)F] · 0.5H2O (IV), have been synthesized, and their crystallographic characteristics have been determined. All the compounds crystallize in monoclinic system, space group P21/c, with the unit cell parameters a = 13.1744(5) Å, b = 9.4598(3) Å, c = 13.0710(4) Å, β = 103.746(1)°, Z = 4, R = 0.0235 (I); a = 13.5902(7) Å, b = 9.5022(4) Å, c = 13.2271(6) Å, β = 102.914(2)°, Z = 4, R = 0.0247 (II); a = 24.7724(8) Å, b = 12.6671(4) Å, c = 9.4464(3) Å, β = 97.661(1)°, Z = 8, R = 0.0448 (III); a = 25.725(1) Å, b = 12.8261(5) Å, c = 9.4929(4) β = 97.208(1)°, Z = 8 (IV). The pairs of compounds I and II and compounds III and IV are isostructural. Crystals of compounds I–III have been subjected to complete X-ray diffraction study. It has been established that the structures of compounds I–III are built of [UO2(CrO4)F]nn− layers, which are parallel to the (100) plane and linked into a framework by alkali-metal cations located between layers, together with water molecules. The effect of topological and geometric isomerism on the structural features of 34 known uranyl compounds of the AT3M2 crystallochemical group, to which the studied compounds I–III also belong, is discussed. More... »

PAGES

788-797

References to SciGraph publications

  • 1982-03. Die Kristallstruktur des Johannits, Cu(UO2)2(OH)2(SO4)2·8H2O in TSCHERMAKS MINERALOGISCHE UND PETROGRAPHISCHE MITTHEILUNGEN
  • 2011-08. An X-ray diffraction study of Rb[UO2(SeO4)F]·H2O in RADIOCHEMISTRY
  • 2010-05. Synthesis and structure of Cs[UO2(SeO4)(OH)] · nH2O (n = 1.5 or 1) in CRYSTALLOGRAPHY REPORTS
  • 2008-03. Maximum filling principle and sublattices of actinide atoms in crystal structures in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
  • 2002-07. Crystal Structure of Rb[UO2(SO4)F] in RADIOCHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1134/s003602361408018x

    DOI

    http://dx.doi.org/10.1134/s003602361408018x

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1050315598


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