anti-syn and anti-anti coordination of the bridging CO32− group in [Cu2(Phen)4(μ-CO3)]B10H10 binuclear complexes: Synthesis, structure, and magnetic properties View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-12-29

AUTHORS

A. E. Dziova, V. V. Avdeeva, I. N. Polyakova, E. A. Malinina, A. V. Rotov, N. N. Efimov, E. A. Ugolkova, V. V. Minin, N. T. Kuznetsov

ABSTRACT

A redox reaction that occurs in the [Cu2B10H10]/Phen system in CH3CN/DMSO and CH3CN/DMF in air yields a Cu(II) binuclear complex, [(Phen)2Cu(CO3)Cu(Phen)2]2+. The [Cu2(Phen)4(μ-CO3)]B10H10 · 2.5DMSO · 2H2O (I) and [Cu2(Phen)4(μ-CO3)]B10H10 · 4DMF (II) compounds have been isolated and studied by X-ray crystallography at 150 K and EPR at 295 K. Their magnetic properties have been studied in the range 300–2 K. In the cations of both compounds, the bridging CO32− group is bidentately coordinated to two Cu atoms. The cations in I and II have different spatial orientations of the Cu-O bonds: anti-syn and anti-anti, respectively. Compound I has weak magnetic interactions caused by a short Cu…Cu distance (4.441 Å) in the dimer. No exchange coupling is observed in II. More... »

PAGES

1527-1535

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023614010045

DOI

http://dx.doi.org/10.1134/s0036023614010045

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1018721928


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