Iron(II) closo-borate complexes with 1,2,4-triazole derivatives: Spin crossover in the iron(II) closo-borate complexes with tris(pyrazol-1-yl)methane View Full Text


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Article Info

DATE

2013-06

AUTHORS

O. G. Shakirova, V. A. Daletskii, L. G. Lavrenova, S. V. Trubina, S. B. Erenburg, K. Yu. Zhizhin, N. T. Kuzhetsov

ABSTRACT

Methods of synthesis of iron(II) complexes containing cluster closo-borate anions—[Fe(Htrz)3]B10Cl10 (I) (HTrz is 1,2,4-triazole), [Fe(NH2Trz)3]B10Cl10 · 2H2O (II) (NH2Trz is 4-amino-1,2,4-triazole), [Fe{HC(pz)3}2]B10Cl10 (III), [Fe{HC(pz)3}2]B10H10 (IV), and [Fe{HC(pz)3}2]B12H12 · 2H2O (V) (HC(pz)3 is tris(pyrazol-1-yl)methane)—have been developed. The compounds have been studied by the static magnetic susceptibility method (78–500 K) and electronic, IR, and EXAFS spectroscopy. Complexes I and II in the temperature range under consideration remain in the high-spin state. Low-spin complex III shows incomplete spin crossover and decomposes on heating above 440 K. Complexes IV and V are characterized by reversible spin crossover 1A1 ⇔ 5T2 accompanied by thermochromism (the pink ⇔ white color change). The crossover temperature (Tc) for IV and V is 375 and 405 K, respectively. More... »

PAGES

650-656

References to SciGraph publications

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  • 2010-04. Spin crossover in iron(II) complexes with tris(pyrazol-1-yl)methane in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
  • 2001-05. Decahydro-closo-decaborate Anion B10H2–10as an Acido Lidand in Copper(I) Complexes in DOKLADY CHEMISTRY
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  • 2004-04. Iron(II) Complexes with 4-R-1,2,4-Triazoles (R = Ethyl, Propyl, Isopropyl): Synthesis and Properties in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
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    http://scigraph.springernature.com/pub.10.1134/s0036023613060211

    DOI

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