Synthesis and crystal structure of lanthanum(III) Iodomercurate(II) complexes with ɛ-Caprolactam View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-05

AUTHORS

A. V. Tikhomirova, E. V. Peresypkina, A. V. Virovets, T. G. Cherkasova

ABSTRACT

The X-ray diffraction study of the crystalline products of the reaction between potassium tetraiodomercurate(II), ɛ-caprolactam, and lanthanum(III) nitrate at a ratio of 3: 16: 2 in an aqueous solution has shown the presence of the following three new crystalline compounds: [LaCpl8]2[HgI4]3 (I), [LaCpl8][HgI4]I3 (II), and [LaCpl7(H2O)]2[HgI4]2[Hg2I6] (III), where Cpl is ɛ-caprolactam ɛ-C6H11NO. Compounds I and II crystallize in tetragonal crystal system, space groups P42/n and , respectively. For compound I, a = 18.59320(10) Å, c = 19.5782(3) Å, V = 6738.32(12) Å3, Z = 2, and ρcalc = 2.067 g/cm3. For compound II, a = 13.2245(10) Å, c = 20.0310(3) Å, V = 3503.17(6) Å3, Z = 2, ρcalc = 2.022 g/cm3. The crystals of compound III are monoclinic (space group P21/n, a = 20.1202(6) Å, b = 14.0569(4) Å, c = 46.3228(12) Å, β = 93.4770(10)°, V = 13077.3(6) Å3, Z = 4, ρcalc = 2.274 g/cm3). [La(Cpl)8]2[Hg2I6]3 (IV), a new double ionic complex salt, has also been synthesized and studied by X-ray diffraction. The crystals of compound IV are triclinic (space group , a = 12.5021(3) Å, b = 14.6436(3) Å, c = 21.4695(4) Å, α = 84.2300(10)°, β = 87.2230(10)°, γ = 74.9970(10)°, V = 3776.30(14) Å3, Z = 1, ρcalc = 2.452 g/cm3). All complexes have a dicrete ionic structure, and the nearest surrounding of a La atom is distorted square-prismatic or trigonal-dodecahedral. The crystal packing of cations is distorted face-centered cubic (I and II) or body-centered cubic (III and IV) with anions located in its cavities. More... »

PAGES

534-542

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023613050215

DOI

http://dx.doi.org/10.1134/s0036023613050215

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1027310202


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