Reaction of trans-[RuNO(NH3)4(OH)]Cl2 with nitric acid and synthesis of ammine(nitrato)nitrosoruthenium complexes View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-08

AUTHORS

E. V. Kabin, V. A. Emel’yanov, V. A. Vorob’yev, N. I. Alferova, S. V. Tkachev, I. A. Baidina

ABSTRACT

The reaction of trans-[RuNO(NH3)4(OH)]Cl2 with nitric acid has been studied. Reaction products have been identified by IR spectroscopy, NMR, mass spectrometry, powder and single-crystal X-ray diffraction, and chemical analysis. Synthesis methods have been developed for amminenitrosoruthenium complexes containing outer-sphere and coordinated nitrate ions: trans-[RuNO(NH3)4(H2O)](NO3)3 (I), trans-[RuNO(NH3)4(NO3)](NO3)2 (II), and fac-[RuNO(NH3)2(NO3)3] (III). Complex II has two polymorphs: monoclinic and tetragonal. The latter has been studied by X-ray crystallography. More... »

PAGES

1146-1153

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023612050105

DOI

http://dx.doi.org/10.1134/s0036023612050105

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1035564412


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