Synthesis, molecular and crystal structure, magnetic properties, luminescence, and solid-phase thermolysis of binuclear Ln(III) pivalates with 2,2′-dipyridyl and 1,10-phenanthroline molecules View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2009-05

AUTHORS

Zh. V. Dobrokhotova, I. G. Fomina, G. G. Aleksandrov, Yu. A. Velikodnyi, V. N. Ikorskii, A. S. Bogomyakov, L. N. Puntus, V. M. Novotortsev, I. L. Eremenko

ABSTRACT

Methods of synthesis of binuclear pivalate complexes L2Ln2(μ-O,η2-OOCCMe3)2(μ2-O,O′-OOCCMe3)2(η2-OOCCMe3)2, where Ln = Sm, Eu, Gd, or Er and L = 2,2′-dipyridyl (Bipy) or 1,10-phenanthroline (Phen), from the corresponding binuclear complexes Ln2(μ2-OOCCMe3)4(OOCCMe3)2(HOOCCMe3)6 · HOOCCMe3(I–IV), as well as of coordination polymers {Ln(OOCCMe3)3}n, were suggested. The compounds were characterized by X-ray crystallography and X-ray powder diffraction and their magnetic properties, solid-phase thermolysis, and the phase composition of solid decomposition products were studied. The structures of the metal carboxylate core and surrounding ligands were shown to have an effect on the thermal stability of the complexes. The luminescence properties of the Eu(III) complexes were analyzed. More... »

PAGES

668-685

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023609050040

DOI

http://dx.doi.org/10.1134/s0036023609050040

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1050662067


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31 schema:description Methods of synthesis of binuclear pivalate complexes L2Ln2(μ-O,η2-OOCCMe3)2(μ2-O,O′-OOCCMe3)2(η2-OOCCMe3)2, where Ln = Sm, Eu, Gd, or Er and L = 2,2′-dipyridyl (Bipy) or 1,10-phenanthroline (Phen), from the corresponding binuclear complexes Ln2(μ2-OOCCMe3)4(OOCCMe3)2(HOOCCMe3)6 · HOOCCMe3(I–IV), as well as of coordination polymers {Ln(OOCCMe3)3}n, were suggested. The compounds were characterized by X-ray crystallography and X-ray powder diffraction and their magnetic properties, solid-phase thermolysis, and the phase composition of solid decomposition products were studied. The structures of the metal carboxylate core and surrounding ligands were shown to have an effect on the thermal stability of the complexes. The luminescence properties of the Eu(III) complexes were analyzed.
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