Synthesis and study of Iron(II) perrhenate complexes with 4-propyl-1,2,4-triazole exhibiting 1A1 ⇄ 5T2 spin transition View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2007-01

AUTHORS

M. B. Bushuev, L. G. Lavrenova, Yu. G. Shvedenkov, A. V. Virovets, L. A. Sheludyakova, S. V. Larionov

ABSTRACT

Coordination compounds of iron(II) perrhenate with 4-propyl-1,2,4-triazole (L), [Fe3L6(ReO4)4(H2O)2](ReO4)2(I), [Fe3L6(H2O)6](ReO4)6·H2O(II), and FeL3(ReO4)2(III), were synthesized. Compounds I and III were studied by static magnetic susceptibility measurements and by IR and electronic spectroscopy. These complexes exhibit a reversible 1A1 ⇄ 5T2 spin transition and thermochromism. Compound I exhibits a spin transition without hysteresis at 185 K. The temperatures of forward and reverse transition for III are 250 and 244 K, respectively. Complex II isolated by crystallization from an acidified aqueous solution of compound I has a linear trinuclear structure of the cation (X-ray diffraction data). The structure of complex I was assumed to be similar, while compound III has a polymeric structure. More... »

PAGES

46-51

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0036023607010093

DOI

http://dx.doi.org/10.1134/s0036023607010093

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1012846851


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