Synthesis and physicochemical characterization of palladium-cerium oxide catalysts for the low-temperature oxidation of carbon monoxide View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2009-11

AUTHORS

E. M. Slavinskaya, A. I. Boronin, I. G. Danilova, Yu. I. Amosov, A. S. Ivanova, P. A. Kuznetsov, I. A. Polukhina, R. V. Gulyaev, A. I. Stadnichenko, S. V. Koshcheev, V. I. Zaikovskii, A. S. Noskov

ABSTRACT

The effect of CeO2 preparation procedure on the electronic and structural states of the active component of Pd/CeO2 catalysts and their activity in the low-temperature reaction of CO oxidation was studied. The following two nonequivalent states of palladium were detected in the catalysts having low-temperature activity using XPS and IR spectroscopy: Pd0(Pdδ+) as the constituent of a palladium-reduced interaction phase and Pd2+ as the constituent of a palladium-oxidized interaction phase PdxCeO2 −δ. It was found that the procedure used for preparing a CeO2 support considerably affected the formation of these phases and quantitative ratios between them. It was demonstrated that the palladium-oxidized interaction phase was responsible for low-temperature activity, whereas the palladium-reduced interaction phase was responsible for activity in the region of medium and high temperatures. More... »

PAGES

819

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0023158409060044

DOI

http://dx.doi.org/10.1134/s0023158409060044

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1007678162


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