Physicochemical and catalytic properties of systems based on CeO2 View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2009-11

AUTHORS

A. S. Ivanova

ABSTRACT

The effect of synthesis conditions, the nature of components, and the ratio between the components on the phase composition, the texture, and the redox and catalytic properties of the Ce-Zr-O, Ce-Zr-M1-O (M1 = Mn, Ni, Cu, Y, La, Pr, or Nd), N/Ce-Zr-O (N = Rh, Pd, or Pt), and Pd/Ce-Zr-M2-O/Al2O3 (M2 = Mg, Ca, Sr, Ba, Y, La, Pr, Nd, or Sm) was considered. A cubic solid solution with the fluorite structure was formed on the introduction of <50 mol % zirconium into CeO2, and the stability of this solid solution depended on preparation procedure and treatment conditions. The presence of transition or rare earth elements in certain concentrations extended the range of compositions with the retained fluorite structure. The texture of the Ce-Zr-O system mainly depended on treatment temperature. An increase in this temperature resulted in a decrease in the specific surface area of the samples. The total pore volume varied over the range of 0.2–0.3 cm3/g and depended on the Ce/Zr ratio. The presence of transition or rare earth elements either increased the specific surface area of the system or made it more stable to thermal treatment. The introduction of the isovalent cation Zr4+ into CeO2 increased the number of lattice defects both on the surface and in the bulk to increase the mobility of oxygen and facilitate its diffusion in the Ce1 − xZrxO2 lattice. The catalytic properties of the Ce-Zr-M1-O or N/Ce-Zr-M2-O systems were due to the presence of anion vacancies and the easy transitions Ce4+ ai Ce3+, M12n+ ai M1n+, and Nδ+ → N0 in the case of noble metals. More... »

PAGES

797-815

References to SciGraph publications

Journal

TITLE

Kinetics and Catalysis

ISSUE

6

VOLUME

50

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0023158409060020

DOI

http://dx.doi.org/10.1134/s0023158409060020

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1009061338


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