Synthesis And Crystal Structure Of Cobalt(Iii) Complexes With Substituted 2-[(Benzimidazole-1-Yl) Iminomethyl]Phenols View Full Text


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Article Info

DATE

2021-12-24

AUTHORS

A. S. Burlov, T. A. Kuzmenko, V. G. Vlasenko, Yu. V. Koshchienko, S. A. Mashchenko, B. V. Chaltsev, A. A. Kolodina, M. A. Kiskin

ABSTRACT

Two Co(III) complexes are synthesized based on 2-{(E)-[2-(hydroxy(alkyl)amino)benzimidazole-1-yl]iminomethyl}phenol (H3L1 and H3L2, alkyl is ethyl or propyl). By the elemental analysis and IR spectroscopy it is established that the obtained complexes have the compositions [Co(H2L1)(HL1)]·2C2H5OH and [Co(H2L2)(HL2)]CH3OH·1/2H2O. Their crystal and molecular structures are determined by single crystal X-ray diffraction (XRD). From the XRD data it is found that the complexes crystallize in the triclinic space group \documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$P\bar{1}$$\end{document} as solvates with alcohol and water molecules. In mononuclear molecules of both complexes, two trischelate ligands in mono- and dianionic forms are coordinated to the Co(III) cation. The coordination environment of the cobalt atom CoN4O2 corresponds to a distorted octahedron in both compounds. More... »

PAGES

1946-1954

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http://scigraph.springernature.com/pub.10.1134/s0022476621120131

DOI

http://dx.doi.org/10.1134/s0022476621120131

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