Mixed-Ligand Iridium(III) Nitro Complexes with Phenantroline View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2019-04

AUTHORS

P. A. Topchiyan, D. B. Vasilchenko, S. V. Tkachev, I. A. Baydina, I. V. Korolkov, D. G. Sheven, S. V. Korenev

ABSTRACT

Interaction of iridium(III) nitro-aqua complexes with 1,10-phenanthroline is studied. Complex anions [Ir(phen)(NO2)4]− and [Ir(phen)(OH)(NO2)3]− are isolated in the solid phase. The complex Na[Ir(phen)(NO2)4](phen)(H2O) is structurally characterized for the first time. Crystallographic data: a=8.0752(5)Ǻ\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$a = 8.0752(5)\acute{\overset{\circ}{\mathrm{A}}}$$\end{document}, b=11.690(7)Ǻ\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$b = 11.690(7)\acute{\overset{\circ}{\mathrm{A}}}$$\end{document}, c=14.012(7)α\documentclass[12pt]{minimal} \usepackage{amsmath} \usepackage{wasysym} \usepackage{amsfonts} \usepackage{amssymb} \usepackage{amsbsy} \usepackage{mathrsfs} \usepackage{upgreek} \setlength{\oddsidemargin}{-69pt} \begin{document}$$c = 14.012(7)\acute{\overset{\circ}{\mathrm{A}}}$$\end{document}, α = 105.55(2)°, β = 91,99(2)°, γ = 103,71(2)° space group P-1, Z = 2, ρcalc = 1,936 g/cm3. The coordination sphere of the iridium atom has a distorted octahedral geometry. The obtained structure contains an island motif consisting of the pairs of complex anions [Ir(phen)(NO2)4]− linked to each other by sodium cations. More... »

PAGES

640-646

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476619040152

DOI

http://dx.doi.org/10.1134/s0022476619040152

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1113946903


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