Synthesis, Ion Mobility, and Phase Transition in the (NH4)6LiHf2Zr2F23 Compound View Full Text


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Article Info

DATE

2018-12

AUTHORS

V. Ya. Kavun, T. F. Antokhina, N. N. Savchenko, M. M. Polyantsev, O. V. Brovkina

ABSTRACT

Ion mobility and a phase transition (PT) in the compound (NH4)6LiHf2Zr2F23 are studied using 1H NMR, 19F NMR, XRD, and DSC methods. The types of ionic motions in the fluoride and ammonium sublattices of this compound are determined at 150–450 K; their activation energies are estimated. It is shown that an order-disorder PT occurs in this compound at 400–450 K to form a metastable high-temperature modification, where ionic motions are represented mainly by the diffusion of fluoride and ammonium ions. More... »

PAGES

1825-1832

References to SciGraph publications

  • 2018-01. Thermal and Transport Properties, Ion Mobility, and Phase Transitions in Compounds (NH4)6CsZr4F23 and (NH4)6CsHf4F23 in RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
  • 2016-06. Phase transitions, ion mobility, and conductivity in fluoro complexes (NH4)6RbZr4F23 and (NH4)6RbHf4F23 in RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
  • 2015-05. Internal mobility, phase transitions, and ionic conductivity in (NH4)6KZr4F23 and (NH4)6KHf4F23 in RUSSIAN JOURNAL OF INORGANIC CHEMISTRY
  • 2005-05. Superionic Conduction in Complex Fluorides of Antimony(III) MnSbxFy (M—Cations of an Alkali Metal, Ammonium, or Thallium, n = 1–3, and x = 1–4) in RUSSIAN JOURNAL OF ELECTROCHEMISTRY
  • 2002-05. Internal Mobility, Phase Transitions, and Ionic Conductivity in Na(NH4)6Zr4F23 and Li(NH4)6Zr4F23 in JOURNAL OF STRUCTURAL CHEMISTRY
  • 1980-07. A study of the anion mobility in mixed fluorides with the tysonite structure in JOURNAL OF STRUCTURAL CHEMISTRY
  • 1999-07. 19F and203,205Tl NMR and structural transformations in chain ammonium and thallium hexafluorozirconates and hexafluorohafnates in JOURNAL OF STRUCTURAL CHEMISTRY
  • 1996-03. Phase transitions and ionic mobility in thallium fluorozirconates in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2013-04. New zirconium fluoride complexes (NH4)6MZr4F23 (M = K, Rb, and Cs): Synthesis and physicochemical properties in RUSSIAN JOURNAL OF COORDINATION CHEMISTRY
  • 2005-05. Ionic Mobility, Phase Transitions, and Superionic Conduction in Solid Solutions (100 − x)PbF2-xZrF4 and Crystals K2ZrF6, (NH4)2ZrF6, KSnZrF7, and M(NH4)6Zr4F23 (M = Li, Na) in RUSSIAN JOURNAL OF ELECTROCHEMISTRY
  • 2009-04. 1H and 19F NMR relaxation time studies in (NH4)2ZrF6 superionic conductor in APPLIED MAGNETIC RESONANCE
  • 2010-10. Ionic mobility and structure of glasses in Zrf4—Bif3—Mf2 (M = Sr, Ba, Pb) systems according to Nmr, Ir, and Raman spectroscopic data in JOURNAL OF STRUCTURAL CHEMISTRY
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    http://scigraph.springernature.com/pub.10.1134/s0022476618080103

    DOI

    http://dx.doi.org/10.1134/s0022476618080103

    DIMENSIONS

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