Nickel Decatungstate [Ni(C2H6SO)5(H2O)]2[W10O32]: Synthesis from a Water-Dimethylsulfoxide Solution, Crystal Structure Determination, IR and Raman Spectroscopic Analysis, Surface Micromorphology View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-01

AUTHORS

E. Yu. Poimanova, A. O. Medved’, S. V. Radio, V. N. Baumer, G. M. Arzumanyan, N. V. Doroshkevich, E. V. Khomutova, E. E. Belousova, G. M. Rozantsev, V. T. Panyushkin

ABSTRACT

Crystalline nickel(II) decatungstate (II) [Ni(C2H6SO)5(H2O)]2[W10O32] is synthesized for the first time and characterized by chemical and thermal analyses, scanning electron microscopy, IR and Raman spectroscopy, and single crystal X-ray diffraction (XRD). By single crystal XRD the crystallographic characteristics of [Ni(C2H6SO)5(H2O)]2[W10O32] are determined (triclinic crystal system, space group P–1, a = 11.9339(7) Å, b = 12.2083(6) Å, c = 12.2083(6) Å, α = 75.235(5)°, β = 71.289(6)°, γ = 87.785(4)°, V = 1692.44(17) Å3 at T = 293(2) K, Z = 1, dx = 3.223 g/cm3) and the structure is found to be composed of isolated [Ni(C2H6SO)5(H2O)]24+ cation complexes and [W10O32]4– anions located in the voids between the cation complexes. By the powder XRD analysis it is shown that the crystals formed by growing from the solution do not contain impurities. More... »

PAGES

145-153

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476618010225

DOI

http://dx.doi.org/10.1134/s0022476618010225

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1101552692


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