X-ray spectroscopy study of lithiated graphite obtained by thermal deposition of lithium View Full Text


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Article Info

DATE

2017-11

AUTHORS

L. L. Lapteva, Yu. V. Fedoseeva, P. N. Gevko, D. A. Smirnov, A. V. Gusel’nikov, L. G. Bulusheva, A. V. Okotrub

ABSTRACT

X-ray photoelectron spectroscopy (XPS), X-ray emission spectroscopy (XES), and near edge X-ray absorption fine structure (NEXAFS) spectroscopy are used for in situ studies of the electronic structure of lithiated natural graphite produced by thermal deposition of lithium upon graphite in a vacuum. By XPS and NEXAFS spectroscopy it is found that lithium vapor thermal deposition results in the formation of a lithiated graphite surface layer and a change in its electronic structure. Based on the quantum chemical simulation of the experimental СKα XES spectrum of lithiated graphite, it is found that lithium atoms are located mostly on the edges of graphite crystallites. Atomic force microscopy reveals that the size of natural graphite flakes varies from 50 nm to 200 nm. More... »

PAGES

1173-1179

References to SciGraph publications

  • 1992. NEXAFS Spectroscopy in NONE
  • Identifiers

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    http://scigraph.springernature.com/pub.10.1134/s0022476617060154

    DOI

    http://dx.doi.org/10.1134/s0022476617060154

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