Crystal structure and EPR spectra of (Bu4N)2[V(dmit)3] View Full Text


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Article Info

DATE

2017-09

AUTHORS

Ya. S. Fomenko, A. L. Gushchin, V. A. Nadolinny, P. A. Abramov, M. N. Sokolov

ABSTRACT

The tris-chelate complex of vanadium(IV) (Bu4N)2[V(dmit)3] is prepared from VCl3 and (Bu4N)2[Zn(dmit)2] (dmit = isotrithionedithiolate C3S52–) and characterized by single crystal XRD and mass spectrometry. The complex crystallizes in the space group Pna21 and has a distorted octahedral environment of vanadium. The complex is paramagnetic and gives a characteristic EPR spectrum in both solution and solid phase. The g factors and hyperfine interaction constants are determined. More... »

PAGES

964-969

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476617050158

DOI

http://dx.doi.org/10.1134/s0022476617050158

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1092329132


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