In situ X-ray spectroscopic investigation of thermal decomposition of double complex salt [Pt(NH3)4][OsCl6] View Full Text


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Article Info

DATE

2017-09

AUTHORS

T. I. Asanova, I. P. Asanov, M.-G. Kim, S. V. Korenev

ABSTRACT

In the paper results of the investigation of the thermal decomposition process of double complex salt [Pt(NH3)4][OsCl6] by x-ray absorption (XAFS) and photoelectron (XPS) spectroscopies have been presented. The data obtained allows a mechanism of the thermal decomposition to be refined. An influence of size effect and nanoalloy formation on chemical shift of Pt and Os is discussed. More... »

PAGES

901-910

References to SciGraph publications

  • 2010-03. Formation of nanosized bimetallic particles based on noble metals in CATALYSIS IN INDUSTRY
  • 2007-05. Synthesis of non-equilibrium PtxOs1−x Solid solutions. Crystal structure of [Pt(NH3)4][OsCl6] in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2008-03. The product of thermobaric treatment of Pt0.25Os0.75 in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2012-05. Double complex salts [Pd(NH3)4]3[Rh(NO2)6]2, [Pd(NH3)4]3[Rh(NO2)6]2·H2O as promising precursors to prepare Pd-Rh nanoalloys in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2013-09-29. On formation mechanism of Pd–Ir bimetallic nanoparticles through thermal decomposition of [Pd(NH3)4][IrCl6] in JOURNAL OF NANOPARTICLE RESEARCH
  • 2005-05. Thermolysis of [Pt(NH3)4][ReHlg6] (Hlg = Cl, Br). Structure refinement for [Pt(NH3)4][ReCl6] in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2004-05. Synthesis of nonequilibrium IrxRe1-x solid solutions. Crystal structure of [Ir(NH3)5Cl]2[ReCl6]Cl2 in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2016-12. PtPd-nanoparticles supported by new carbon materials in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2002-05. Syntheses of [Rh(NH3)5Cl][MCl6] (M = Re, Os, Ir) and Investigation of Their Thermolysis Products. Crystal Structure of [Rh(NH3)5Cl][OsCl6] in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2009-12. X-ray study of the thermolysis products of (NH4)2[OsCl6]x[PtCl6]1−x in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2000-03. Syntheses and X-ray studies of the complexes [M(NH3)4][M′X6] (M = Pt, Pd; M′ = Re, Os; X = Cl, Br) in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2015-09-29. Study on thermal decomposition of double complex salt [Pd(NH3)4][PtCl6] in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1134/s0022476617050079

    DOI

    http://dx.doi.org/10.1134/s0022476617050079

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1092332171


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