Structure and thermal properties of a tungsten sulfide cluster with thiourea ligands View Full Text


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Article Info

DATE

2016-09

AUTHORS

Yu. A. Laricheva, A. L. Gushchin, P. A. Abramov, M. N. Sokolov

ABSTRACT

The reaction of [W3S4(H2O)9]4+ with thiourea (tu) in hydrochloric acid produces a new cluster complex [W3S4(tu)8(H2O)]Cl4∙2H2O containing coordinated thiourea. The complex is characterized by elemental analysis, thermogravimetry, IR, NMR, UV-Vis spectroscopy, and mass spectrometry. The crystal structure is determined by X-ray analysis. The thermal decomposition of [W3S4(tu)8(H2O)]Cl4∙2H2O on heating from 20°С to 700°С in He gives WS2, identified by the X-ray diffraction pattern. DFT calculations for [W3S4(tu)8(H2O)]4+ show that HOMO has a comparable contribution from metal- and ligand-centered atomic orbitals. More... »

PAGES

962-969

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URI

http://scigraph.springernature.com/pub.10.1134/s0022476616050164

DOI

http://dx.doi.org/10.1134/s0022476616050164

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