Molecular and crystal structure of iron(III) and nickel(II) complexes with 1′-phthalazinylhydrazones of heterocyclic carbonyl compounds View Full Text


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Article Info

DATE

2015-01

AUTHORS

L. D. Popov, S. I. Levchenkov, I. N. Shcherbakov, G. G. Aleksandrov, Z. A. Starikova, V. V. Lukov, V. A. Kogan

ABSTRACT

The structures of iron(III) and nickel(II) complexes with the composition [FeL2]Cl·H2O (1) and [Ni(HL′2)]·DMSO·0.5H2O (2), where L and HL′ are monodeprotonated residues of 1′-phthalazinylhydrazones of 2-acetyl benzimidazole and 1-phenyl-3-methyl-4-formyl-5-hydroxypyrazole respectively, are determined using single crystal X-ray diffraction analysis. Both compounds crystallize in the monoclinic symmetry. The Fe(III) and Ni(II) ions in the complexes have octahedral N6 and N4O2 donor environments respectively. Due to intermolecular hydrogen bonds, the molecules of the complexes form corrugated (complex 1) and linear (complex 2) molecular chains in the crystal. More... »

PAGES

102-107

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s002247661501014x

DOI

http://dx.doi.org/10.1134/s002247661501014x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1036764804


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