Crystal structure of the ionic cluster complex (2,2′-bipyH2)2[Re4Se4(CN)12]·(2,2′-bipy)·7H2O View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-09

AUTHORS

Ya. M. Gaifulin, A. I. Smolentsev, Yu. V. Mironov

ABSTRACT

A rhenium cluster complex (2,2′-bipyH2)2[Re4Se4(CN)12] · (2,2′-bipy)·7H2O (1) is obtained and characterized. The compound crystallizes in a monoclinic space group C2/c with the unit cell parameters: a = 16.9191(6) Å, b = 18.7458(6) Å, c = 19.0139(5) Å, β = 108.568(1)°, V = 5716.6(3) Å3, Z = 4, dx = 2.291 g/cm3. The crystal structure is a packing of bipyridylium cations (2,2′-bipyH2)2+, cluster anions [Re4Se4(CN)12]4−, bipyridyl molecules, and crystal water molecules, which are linked together by a system of hydrogen bonds. More... »

PAGES

920-922

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476614050187

DOI

http://dx.doi.org/10.1134/s0022476614050187

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1038045523


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