Structural study of complex [Rh(NH3)5(NO2)](NO3)2·H2O, [Rh(NH3)5(NO2)][Pd(NO2)4], and K2[Rh(NH3)(NO2)5]·H2O salts View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-05

AUTHORS

I. A. Baidina, A. I. Smolentsev, A. V. Belyaev

ABSTRACT

Compounds [Rh(NH3)5(NO2)](NO3)2·H2O (I) with a = 7.6230(3) Å, b = 7.6230(3) Å, c = 10.3584(4) Å, space group I-42m, Z = 2, dcalc = 2.026 g/cm3, V = 601.93(4) Å3, Rh-NH3 eq = 2.074 Å, Rh-NH3 ax (NO2) = 2.048 Å; [Rh(NH3)5(NO2)][Pd(NO2)4] (II) with a = 8.095(3) Å, b = 22.422(8) Å, c = 7.887(3) Å, β = 98.559(17)°, space group Cc, Z = 4, dcalc = 2.461 g/cm3, V = 1415.6(9) Å3, Rh-NH3 eq = 2.069 Å, Rh-NH3 ax = 2.090 Å, Rh-NO2 = 2.002 Å; K2[Rh(NH3)(NO2)5]·H2O (III) with a = 7.5177(5) Å, b = 20.9856(15) Å, c = 7.7017(5) Å, space group Cmc21, Z = 4, dcalc = 2.439 g/cm3, V = 1215.05(14) Å3, Rh-NH3 ax (NO2) = 2.094 Å, Rh-NO2 eq = 2.030 Å are synthesized and studied using single crystal X-ray diffraction. More... »

PAGES

503-508

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476614030172

DOI

http://dx.doi.org/10.1134/s0022476614030172

DIMENSIONS

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