Structure of [Dy(Phen)(C4H8NCS2)3]·3CH2Cl2 solvate. Magnetic properties and photoluminiscence of [Ln(Phen)(C4H8NCS2)3] (Ln = Sm, Eu, Tb, Dy, Tm) complexes View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-03

AUTHORS

Yu. A. Bryleva, L. A. Glinskaya, I. V. Korol’kov, A. S. Bogomyakov, M. I. Rakhmanova, D. Yu. Naumov, T. E. Kokina, S. V. Larionov

ABSTRACT

It is found that diffraction patterns of complexes I–V of the composition [Ln(Phen)(C4H8NCS2)3] (Ln = Sm, Eu, Tb, Dy, and Tm respectively) are similar. Single crystals of [Dy(Phen)(C4H8NCS2)3]·3CH2Cl2 (VI) obtained are. According to the X-ray crystallographic data, in the structure of VI the unit cell contains two crystallographically independent molecules of the [Dy(Phen)(C4H8NCS2)3] complex and six CH2Cl2 molecules. The N2S6 coordination polyhedron of the Dy atom is a distorted square antiprism. In the range of 2–300 K the magnetic properties of complexes I–V are studied. It is found that complex III passes to the magnetically ordered state; the spontaneous magnetization at 2 K is 24 600 G·cm3/mol. At 300 K compounds I–IV exhibit photoluminescence in the visible spectral range. It is found that the photoluminescence intensity of complex I is several times higher than the photoluminescence intensity of complexes II–IV. More... »

PAGES

319-326

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s002247661402019x

DOI

http://dx.doi.org/10.1134/s002247661402019x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1015291571


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