Structure, synthesis, and thermal properties of trans-[Ru(NO)(NH3)4(SO4)]NO3·H2O View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2014-03

AUTHORS

A. N. Makhinya, M. A. Il’in, I. A. Baidina, P. E. Plyusnin, N. I. Alferova, D. P. Pishchur

ABSTRACT

In treatment of trans-[Ru(NO)(NH3)4(OH)]Cl2 with concentrated sulfuric acid on heating trans-[Ru(NO)(NH3)4(SO4)](HSO4)·H2O (I) is obtained with a yield close to quantitative. In the interaction of the saturated solution of I with a saturated NaNO3 solution a trans-[Ru(NO)(NH3)4(SO4)]NO3·H2O (II) precipitate forms whose structure is determined by single crystal XRD: space group P212121, a = 6.8406(3) Å, b = 12.6581(5) Å, c = 13.3291(5) Å. A monodentately coordinated sulfate ion is in the trans-position to the nitroso group. Compound II is characterized by IR spectroscopy, powder XRD, and diffuse reflectance spectroscopy. The process of its thermolysis is studied; by differential scanning calorimetry the thermal effect of the dehydration reaction occurring on heating to 120°C (ΔH = 58.9 ± 1.5 kJ/mol) is estimated. The final product of the thermolysis of II is a mixture of Ru and RuO2. More... »

PAGES

311-318

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476614020188

DOI

http://dx.doi.org/10.1134/s0022476614020188

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1043138731


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