Double complex salts [Pd(NH3)4]3[Rh(NO2)6]2, [Pd(NH3)4]3[Rh(NO2)6]2·H2O as promising precursors to prepare Pd-Rh nanoalloys View Full Text


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Article Info

DATE

2012-05

AUTHORS

A. A. Rybinskaya, P. E. Plyusnin, E. A. Bykova, S. A. Gromilov, Yu. V. Shubin, S. V. Korenev

ABSTRACT

Two new double complex salts [Pd(NH3)4]3[Rh(NO2)6]2 (I) and [Pd(NH3)4]3[Rh(NO2)6]2·H2O (II) are synthesized and characterized. The techniques to produce one-phase residues of the salts are developed. The crystallographic data for I: a = 18.915(2) Å, V = 6767.4 Å3, F-43c space group, Z = 8, dx = 2.548 g/cm3; II: a = 21.160(6) Å, b = 8.085(7) Å, c = 21.363(4) Å, β = 91.71(4)°, V = 3661.1(6) Å3, P21/c space group, dx = 2.357 g/cm3. Thermal properties of the obtained compounds in the hydrogen and helium atmosphere are studied. It is shown that the final product of their decomposition both in the inert and reducing atmosphere is a powder consisting of bimetallic nanosized particles (nanoalloy) of Pd0.59Rh0.41 (Fm-3m space group, a = 3.856(2) Å, crystallite size of 8–11 nm). More... »

PAGES

527-533

References to SciGraph publications

  • 2011-08. Crystal structure of [Pd(NH3)4]3[Ir(NO2)6]2·H2O in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2010-08. Refinement of the (NH4)2Na[Rh(NO2)6] Crystal Structure in JOURNAL OF STRUCTURAL CHEMISTRY
  • 1994-04. The Pd-Rh (Palladium-Rhodium) system in JOURNAL OF PHASE EQUILIBRIA AND DIFFUSION
  • 2009-11-15. Size and shape effects on the order–disorder phase transition in CoPt nanoparticles in NATURE MATERIALS
  • 2002-07. Binary Complexes [M(NH3)5Cl][PdCl4] · H2O (M = Rh, Co): Crystal Structure of [Rh(NH3)5Cl][PdCl4] · H2O in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2011-06. Crystal structure of [Pd(NH3)4][Rh(NH3)(NO2)5] in JOURNAL OF STRUCTURAL CHEMISTRY
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    URI

    http://scigraph.springernature.com/pub.10.1134/s002247661203016x

    DOI

    http://dx.doi.org/10.1134/s002247661203016x

    DIMENSIONS

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