Structure of complex salts [Co(NH3)6][Rh(NO2)6] and [Co(NH3)6][(NO2)3Rh(μ-NO2)1+x(μ-OH)2−xRh(NO2)3]·(2-x)(H2O), x = 0.17 View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-05

AUTHORS

A. I. Gubanov, N. V. Kuratieva, E. Yu. Filatov, S. V. Korenev

ABSTRACT

The structures of two salts [Co(NH3)6][Rh(NO2)6] (I) and [Co(NH3)6][(NO2)3Rh(μ-NO2)1+x(μ-OH)2−x Rh(NO2)3]·(2−x)(H2O), x = 0.17 (II) are solved. Single crystals of the salts are obtained by the counter diffusion method through the gel of aqueous solutions of [Co(NH3)6]Cl3 and Na3[Rh(NO2)6]. The structure of [Co(NH3)6][Rh(NO2)6] is consistent with the diffraction data for a polycrystalline sample of poorly soluble fine salt formed in the exchange reaction between aqueous solutions of [Co(NH3)6]Cl3 and Na3[Rh(NO2)6]. The structure of [Co(NH3)6][(NO2)3Rh(μ-NO2)1+x(μ-OH)2−xRh(NO2)3]·(2−x)(H2O), x = 0.17 exhibits the stabilizing effect of a large cation in the formation of novel, unknown previously coordination ions: [(NO2)3Rh(μ-NO2)(μ-OH)2Rh(NO2)3]3− and [(NO2)3Rh(μ-NO2)2(μ-OH)Rh(NO2)3]3−. More... »

PAGES

503-508

References to SciGraph publications

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  • 2010-06. [Rh(NH3)5Cl]WO4 crystal structure in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2009-12. Crystal structure of [Cu(NH3)4](ReO4)2 in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2007-03. Co-Pt bimetallic catalysts for the selective oxidation of carbon monoxide in hydrogen-containing mixtures in KINETICS AND CATALYSIS
  • 2010-12-16. Bimetallic Rh-Co/ZrO2 catalysts for ethanol steam reforming into hydrogen-containing gas in KINETICS AND CATALYSIS
  • 2010-10. X-ray diffraction study of [MI(NH3)5Cl] [MIIBr6] (MI = Rh, Ir; MII = Re, Ir) polycrystals in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2010-08. Structure and Thermal Properties of [Rh(NH3)5Cl](WO4)x(MoO4)1s-x (x = 0, 0.5, 1) in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2010-06. two crystalline modifications of [Au(dien)Cl](ReO4)2: synthesis, structure, and thermal properties in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2009-10. EPR study of solid solutions of [Cr(NH3)5Cl]x[Rh(NH3)5Cl]1−x[PdCl4]·nH2O and [Cr(NH3)5Cl]x[Rh(NH3)5Cl]1−x[PtCl4] compounds in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2010-02. First example of ruthenium nitroso monoammine complex. Crystal structure of [Ru(NO)(NH3)3(H2O)Cl] × [Ru(no)(NH3)3(OH)Cl][Ru(NO)(NH3)Cl4]2Cl·2H2O in JOURNAL OF STRUCTURAL CHEMISTRY
  • 2010-03-19. XAFS investigation of [Pd(NH3)4][AuCl4]2 and its thermolysis products in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
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    DOI

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