Synthesis and structure investigation of Co(III) complex salts with the perrhenate anion View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2012-02

AUTHORS

I. A. Baidina, E. Yu. Filatov, E. V. Makotchenko, A. I. Smolentsev

ABSTRACT

Complex salts of the composition [Co(NH3)6](ReO4)3·2H2O (I), [Co(en)3](ReO4)3 (II), [Co(NH3)5H2O](ReO4)3·2H2O (III), and [Co(NH3)5Cl](ReO4)2·0.5H2O (IV) are obtained. Their crystal structures are determined by single crystal XRD. Crystallographic characteristics: (I) a = 9.9797(3) Å, b = 12.6994(3) Å, c = 14.7415(4) Å, β = 102.870(1)°, C2/c space group; (II) a = 8.0615(3) Å, b = 8.4483(4) Å c = 8.8267(4) Å, α = 61.923(2)°, β = 89.552(2)°, γ = 72.295(2)°, P1 space group; (III) a = 8.0086(4) Å, b = 12.9839(6) Å, c = 17.5122(7) Å, β=91.858(1)°, P21/n space group; (IV) a = 14.9446(3) Å, b = 14.6562(4) Å, c = 12.2434(4) Å, Cmc21 space group. More... »

PAGES

112-118

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476612010143

DOI

http://dx.doi.org/10.1134/s0022476612010143

DIMENSIONS

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