Crystal structure of a silver(I) complex {[Ag(N-methylthiourea)2]NO3}n exhibiting infinite chains of AgS4 tetrahedra View Full Text


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Article Info

DATE

2011-02

AUTHORS

H. Ur Rehman, S. Ahmad, H. Ajaz, M. Hanif, M. Altaf, H. Stoeckli-Evans

ABSTRACT

A polymeric silver(I) complex, bis(N-methylthiourea)silver(I) nitrate, {[Ag(Metu)2]NO3}n is prepared and its crystal structure is determined. The compound crystallizes in the monoclinic C2/c space group. In the structure, distorted AgS4 tetrahedra are linked through the sulfur atoms of the Metu ligand to form isolated infinite chains of the type [Ag(SR)2]nn+. The cationic chains are separated from each other by nitrate ions that do not coordinate to the metal ion. The chains are bridged via N-H...O hydrogen bonds involving the nitrate ions. The complex exhibits an Ag—Ag separation of ∼3.21 Å indicating the existence of significant argentophilic interactions. An upfield shift in the >C=S resonance of Metu in 13C NMR and downfield shift in the N-H resonance in 1H NMR are consistent with sulfur coordination to silver(I). More... »

PAGES

160

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0022476611010215

DOI

http://dx.doi.org/10.1134/s0022476611010215

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1021940317


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