Order–Disorder Structural Transformations in Nanocrystalline Highly Imperfect Gd2MO5 (M = Zr and Hf) Fluorite Derivatives View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2018-03-14

AUTHORS

L. P. Lyashenko, L. G. Shcherbakova, I. I. Tartakovskii, A. A. Maksimov, R. D. Svetogorov, Ya. V. Zubavichus

ABSTRACT

Order–disorder phenomena in nanocrystalline Gd2ZrO5 and Gd2HfO5 with highly imperfect fluorite- derived structures in the range 1000–1600°C have been studied using monochromatic synchrotron X-ray diffraction and Raman spectroscopy. The results demonstrate that the synthesis process leads to the formation of two coherent phases identical in composition: a nanocrystalline disordered fluorite-like (F) phase (Fm3m) and a nanoparticulate ordered fluorite derivative (C1) (Ia3). Their lattice parameters have been determined. In the range 1000–1600°C, the Raman spectra of the Gd2ZrO5 and Gd2HfO5 materials contain broad bands in low- and high-frequency regions, at ~118 (108), 362 (353), and 670 (665) cm–1, which characterize the C1 and F phases, respectively. More... »

PAGES

245-252

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0020168518030093

DOI

http://dx.doi.org/10.1134/s0020168518030093

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1101527927


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