High-pressure phase transformations, microstructure, and magnetic properties of the hypereutectic alloy 10Ni-90Al View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2013-11

AUTHORS

A. G. Padalko, O. G. Ellert, N. N. Efimov, V. M. Novotortsev, G. V. Talanova, G. I. Zubarev, V. T. Fedotov, A. N. Suchkov, K. A. Solntsev

ABSTRACT

Phase transformations of the hypereutectic alloy 10Ni-90Al have been studied by differential barothermal analysis at temperatures of up to 900°C and pressures of up to ≅100 MPa. We have determined the pressure coefficients of the liquidus and solidus temperatures and the temperatures of solid-state dissolution and precipitation of the intermetallic phase Al3Ni. At high pressures, the solid-state decomposition of the supersaturated solid solution of nickel in aluminum occurs at 622°C and yields an (Al) + Al3Ni mixture. We assume that, during cooling of the alloy at high pressure, intermetallic particles form in three steps. Barothermal analysis data have been compared to the canonical t-x phase diagram of the Al-Ni system. As a result of melting and crystallization at high pressure, the microcrystalline structure of the as-prepared alloy transforms to a macrocrystalline, dendritic structure and the micropore concentration increases. X-ray diffraction data indicate an increase in the unit-cell volumes of the Al and Al3Ni in the alloy crystallized at 100MPa. We have studied the magnetic properties of the alloy after barothermal analysis. More... »

PAGES

1098-1105

Journal

TITLE

Inorganic Materials

ISSUE

11

VOLUME

49

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0020168513110125

DOI

http://dx.doi.org/10.1134/s0020168513110125

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1001568498


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