A comparative study of graphene materials formed by thermal exfoliation of graphite oxide and chlorine trifluoride-intercalated graphite View Full Text


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Article Info

DATE

2013-11

AUTHORS

Yu. M. Shul’ga, A. S. Lobach, S. A. Baskakov, N. G. Spitsyna, V. M. Martynenko, A. V. Ryzhkov, V. B. Sokolov, K. I. Maslakov, A. P. Dement’ev, A. V. Eletskii, V. A. Kazakov, S. K. Sigalaev, R. N. Rizakhanov, N. Yu. Shul’ga

ABSTRACT

Graphene 3D materials GM1 and GM2 obtained by explosive exfoliation of graphite oxide and graphite intercalated with chlorine trifluoride, respectively, have been studied by elemental analysis, X-ray photoelectron spectroscopy, mass spectrometry, infrared and Raman spectroscopy, and scanning electron microscopy. The specific surface area, the pore size, and electrical conductivity of the materials have been measured. A comparative study has shown that the gas mixture produced during the preparation of GM1 is less hazardous than that in the case of GM2. However, GM2 exhibits a higher conductivity and a larger size of graphene crystallites. The feasibility of isolation of a suspension of graphene nanosheets from the test 3D materials has been demonstrated. Possible applications of these materials are discussed. More... »

PAGES

331-338

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s001814391306009x

DOI

http://dx.doi.org/10.1134/s001814391306009x

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1001477836


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30 schema:description Graphene 3D materials GM1 and GM2 obtained by explosive exfoliation of graphite oxide and graphite intercalated with chlorine trifluoride, respectively, have been studied by elemental analysis, X-ray photoelectron spectroscopy, mass spectrometry, infrared and Raman spectroscopy, and scanning electron microscopy. The specific surface area, the pore size, and electrical conductivity of the materials have been measured. A comparative study has shown that the gas mixture produced during the preparation of GM1 is less hazardous than that in the case of GM2. However, GM2 exhibits a higher conductivity and a larger size of graphene crystallites. The feasibility of isolation of a suspension of graphene nanosheets from the test 3D materials has been demonstrated. Possible applications of these materials are discussed.
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