Phase composition and structure of sodium aluminophosphate based glass materials depending on their synthesis conditions View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-02

AUTHORS

S. V. Stefanovsky, O. I. Stefanovskaya, M. I. Kadyko, M. B. Remizov, P. V. Kozlov, E. A. Belanova, B. F. Myasoedov

ABSTRACT

The effect of the method of synthesis on the structure of aluminophosphate glasses intended for immobilization of high level waste from uranium–graphite channel reactor spent nuclear fuel reprocessing has been studied by X-ray powder diffraction and Fourier transform IR spectroscopy. Slow cooling in a furnace, both spontaneous cooling in a switched-off furnace and cooling simulating the conditions of glass cooling in their disposal canisters, or additional heat treatment (annealing) led to partial crystallization of glasses with segregation of different modifications of aluminum orthophosphate. For orthoand pyrophosphate based glasses with similar anionic motifs, their phase composition and degree of crystallization depend not so much on the chemical composition of a sample as on its heat treatment history. More... »

PAGES

32-36

Journal

TITLE

Doklady Physical Chemistry

ISSUE

2

VOLUME

466

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0012501616020020

DOI

http://dx.doi.org/10.1134/s0012501616020020

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1012325882


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