Synthesis and structure of 1-[(3-hydroxybenzo[b]thiophen-2-yl)methylidene]-3-oxo-5-phenyl-1-pyrazolidinium-2-ide View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2016-11

AUTHORS

O. S. Popova, V. A. Bren’, V. V. Tkachev, A. N. Utenyshev, Yu. V. Revinskii, K. S. Tikhomirova, V. P. Rybalkin, A. G. Starikov, G. S. Borodkin, A. D. Dubonosov, G. V. Shilov, S. M. Aldoshin, V. I. Minkin

ABSTRACT

Potentially tautomeric azomethine imine, 1-[(3-hydroxybenzo[b]thiophen-2-yl)methylidene]-3-oxo-5-phenyl-1-pyrazolidinium-2-ide has been prepared. According to X-ray diffraction, 1H, 13C, and 15N NMR and electronic spectroscopy, the compound exists as 3-hydroxybenzothiophene structure containing intermolecular hydrogen bond between the hydroxy group and the carbonyl oxygen of the pyrazolidone ring in crystal state. Quantum chemical calculations predict the possibility of OH and NH tautomeric forms. More... »

PAGES

311-313

Identifiers

URI

http://scigraph.springernature.com/pub.10.1134/s0012500816110033

DOI

http://dx.doi.org/10.1134/s0012500816110033

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1000627703


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