Comparative Analysis of Boron Powders Obtained by Various Methods. I. Microstructure and Oxidation Parameters during Heating View Full Text


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Article Info

DATE

2018-07

AUTHORS

A. N. Pivkina, N. V. Muravyev, K. A. Monogarov, D. B. Meerov, I. V. Fomenkov, E. A. Skryleva, M. Yu. Presnyakov, A. L. Vasiliev, N. I. Shishov, Yu. M. Milekhin

ABSTRACT

This paper describes a study of boron powders and powder compounds, obtained by various methods, including metallothermal, electrolytic, and borane cracking methods. The crystal state, particle size and microstructure, presence and composition of impurities, and chemical composition of the oxide layer of boron particles are profoundly investigated. The effects of the above-mentioned characteristics on the particle oxidation parameters during heating with a constant rate are analyzed. The determining influence of chemical composition of the particle surface layer on the initial temperature of their intense oxidation is established. It is shown that the maximum increase in the mass and heat release value during oxidation of the boron powders is almost independent of microstructural features, crystal state, and chemical composition of and oxide layer thickness of the particles, and cannot serve as indicators of completeness of boron oxidation during heating. More... »

PAGES

450-460

References to SciGraph publications

  • 1987-02. Laser-induced vapour-phase syntheses of boron and titanium diboride powders in JOURNAL OF MATERIALS SCIENCE
  • 1981-03. Heat-liberation kinetics in boron-oxygen interaction in COMBUSTION, EXPLOSION, AND SHOCK WAVES
  • 2015-04-03. Ignition and combustion characteristics of compound of magnesium and boron in JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY
  • 1992-07. Hydrogen, nitrogen, and oxygen behavior in boron in JOURNAL OF MATERIALS RESEARCH
  • 2003-02. Amorphous boron nanoparticles and BN encapsulating boron nano-peanuts prepared by arc-decomposing diborane and nitriding in JOURNAL OF MATERIALS SCIENCE
  • 1974-07. Ignition of a solid particle of boron in COMBUSTION, EXPLOSION, AND SHOCK WAVES
  • 1992-01. Combustion of boron-containing condensed systems in COMBUSTION, EXPLOSION, AND SHOCK WAVES
  • 1976-01. Oxidation kinetics of boron in COMBUSTION, EXPLOSION, AND SHOCK WAVES
  • 2014-11-21. Ignition, combustion, and oxidation of mixtures of amorphous and crystalline boron powders in COMBUSTION, EXPLOSION, AND SHOCK WAVES
  • 2013-12. Structural characterization of electrodeposited boron in BULLETIN OF MATERIALS SCIENCE
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    http://scigraph.springernature.com/pub.10.1134/s0010508218040093

    DOI

    http://dx.doi.org/10.1134/s0010508218040093

    DIMENSIONS

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