Adducts of metallochelate complexes of tridentate N,N,N-donating azomethine ligands: Crystal structures of (2-aminopyridine)[2-N-tosylamino(2′-tosylaminobenzal)anilinato]nickel(II) and (methanol)[2-N-tosylamino(2′-tosylaminobenzal)anilinato]copper(II) View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

2003-05

AUTHORS

D. A. Garnovskii, G. G. Sadikov, A. S. Antsyshkina, A. S. Burlov, I. S. Vasil’chenko, E. D. Garnovskaya, V. S. Sergienko, A. D. Garnovskii

ABSTRACT

The reaction between 2-N-tosylamino-(2′-tosylaminobenzal)aniline (H2L), 2-aminopyridine (L′), and a zero-valent metal (M) in methanol results in the electrochemical synthesis of the ML · L′ adducts [M = Ni (I) or Co]. The copper complex obtained under the same conditions has the composition CuL · CH3OH (II). The structures of the compounds obtained are investigated using IR spectroscopy, FAB+ mass spectrometry, and magnetochemistry. The crystal structures of compounds I and II are determined by X-ray diffraction. In molecules I and II, the metal atoms are coordinated by three N atoms of the L ligand. The mean M-N distances are 1.97 in I and 1.89 Å in II. The fourth site in the coordination sphere of the central atom in I and II is occupied by the endocyclic N atom of the L′ ligand (Ni-N, 2.01 Å) and the O atom of the methanol molecule (Cu-O, 2.06 Å), respectively. The coordination polyhedra of the metal atoms in I and II are complemented by the O atom of the tosyl fragment of the L ligand (Ni-O, 2.41 Å in I; Cu-O, 2.64 Å in II). More... »

PAGES

426-434

References to SciGraph publications

  • 1993. Direct Electrochemical Synthesis of Inorganic and Organometallic Compounds in MOLECULAR ELECTROCHEMISTRY OF INORGANIC, BIOINORGANIC AND ORGANOMETALLIC COMPOUNDS
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