Crystalline-Amorphous-Crystalline Transformation in a Highly Brilliant Luminescent System with Trigonal-Planar Gold(I) Centers View Full Text


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Article Info

DATE

2016-09

AUTHORS

Kosuke Igawa, Nobuto Yoshinari, Mitsutaka Okumura, Hiroyoshi Ohtsu, Masaki Kawano, Takumi Konno

ABSTRACT

Photoluminescent compounds showing emission color changes in response to external stimuli have received considerable attention because of their wide range of applications. Here, we report the unique photoluminescence behavior of a digold(I) coordination system with trigonal-planar Au(I) centers, [Au2(dppm)3](2+) (dppm = bis(diphenylphosphino)methane). This system shows an extremely intense phosphorescence, with a quantum yield of >95% in the solid state. Both the emission color and thermal stability vary due to changing counter ions (Cl(-) vs. OTf(-)). Of particular note is the thermal crystalline-amorphous-crystalline transformation for the chloride salt, which is accompanied by drastic emission color changes. Single-crystal and powder X-ray diffractions demonstrate that the two-step transformation is induced by the loss of water molecules of crystallization with the subsequent removal of a dppm ligand to form [Au2(dppm)2](2+), which is mechanically reverted back to [Au2(dppm)3](2+). More... »

PAGES

26002

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/srep26002

DOI

http://dx.doi.org/10.1038/srep26002

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1050198575

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/27184365


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