Synthesis and Properties Evolution of a Family of Tiara-like Phenylethanethiolated Palladium Nanoclusters View Full Text


Ontology type: schema:ScholarlyArticle      Open Access: True


Article Info

DATE

2015-11-16

AUTHORS

Jishi Chen, Liren Liu, Linhong Weng, Yuejian Lin, Lingwen Liao, Chengming Wang, Jinlong Yang, Zhikun Wu

ABSTRACT

Tiara-like thiolated group 10 transition metal (Ni, Pd, Pt) nanoclusters have attracted extensive interest due to their fundamental scientific significance and potential application in a number of fields. However, the properties (e.g. the absorption) evolution with the ring size’s increase was not investigated so far to our best knowledge, due to the challenge of obtaining a series of nanocluster analogues. Herein, we successfully synthesized, isolated and identified a family of [Pd(SC2H4Ph)2]n nanoclusters (totally 17 novel clusters, n = 4–20). Their structures were determined to be tiara-like by single crystal X-ray crystallography together with theoretical calculation; their formation mechanism was proposed to be a substitution—polycondensation—ring-closure process based on experimental observations. All of these clusters are rather robust (anti-reductive and anti-oxidative) owing to their tiara-like structures with large HOMO-LUMO gaps. Finally, the optical and electrochemical evolution with the increase of ring size was investigated and it is found that both optical and electrochemical gaps have a “turning point” at a size corresponding to n = 8 for [Pd(SR)2]n nanoclusters. More... »

PAGES

16628

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/srep16628

DOI

http://dx.doi.org/10.1038/srep16628

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1047098967

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/26567806


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