Stabilization of metastable ferroelectric Ba1-xCaxTi2O5 by breaking Ca-site selectivity via crystallization from glass View Full Text


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Article Info

DATE

2013-12

AUTHORS

Atsunobu Masuno, Chikako Moriyoshi, Teruyasu Mizoguchi, Toshihiro Okajima, Yoshihiro Kuroiwa, Yasutomo Arai, Jianding Yu, Hiroyuki Inoue, Yasuhiro Watanabe

ABSTRACT

The thermal stability and dielectric and structural properties of ferroelectric Ba1-xCaxTi2O5 (0 ≤ x ≤ 0.30) prepared by crystallization from glass are investigated. The Ba1-xCaxTi2O5 compounds with x < 0.10 are thermally stable phases, while those with x ≥ 0.10 are metastable phases. The ferroelectric transition temperature drastically decreases from 470 to 220°C with increasing x. Crystal structure analyses reveal that one of two possible Ba sites is occupied by Ca in the stable phase region, while Ca-site selectivity is broken in the metastable phase region. The Ca-site selectivity introduces local distortion and makes the crystal lattice unstable. However, the local distortion is suppressed by the occupancy of Ca into both Ba sites. Accordingly, the metastable ferroelectric phase can be obtained beyond the substitution limit of Ca by crystallization from the glassy state. The stabilization mechanism provides possible wide control of the functionality of materials by expanding the composition range. More... »

PAGES

3010

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/srep03010

DOI

http://dx.doi.org/10.1038/srep03010

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1032163615

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/24145958


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