Mechanistic understanding of surface plasmon assisted catalysis on a single particle: cyclic redox of 4-aminothiophenol View Full Text


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Article Info

DATE

2013-12

AUTHORS

Ping Xu, Leilei Kang, Nathan H. Mack, Kirk S. Schanze, Xijiang Han, Hsing-Lin Wang

ABSTRACT

Surface plasmon assisted catalysis (SPAC) reactions of 4-aminothiophenol (4ATP) to and back from 4,4'-dimercaptoazobenzene (DMAB) have been investigated by single particle surface enhanced Raman spectroscopy, using a self-designed gas flow cell to control the reductive/oxidative environment over the reactions. Conversion of 4ATP into DMAB is induced by energy transfer (plasmonic heating) from surface plasmon resonance to 4ATP, where O₂ (as an electron acceptor) is essential and H₂O (as a base) can accelerate the reaction. In contrast, hot electron (from surface plasmon decay) induction drives the reverse reaction of DMAB to 4ATP, where H₂O (or H₂) acts as the hydrogen source. More interestingly, the cyclic redox between 4ATP and DMAB by SPAC approach has been demonstrated. This SPAC methodology presents a unique platform for studying chemical reactions that are not possible under standard synthetic conditions. More... »

PAGES

2997

Identifiers

URI

http://scigraph.springernature.com/pub.10.1038/srep02997

DOI

http://dx.doi.org/10.1038/srep02997

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1024547227

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/24141289


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