Equilibrium p-T Phase Diagram of Boron: Experimental Study and Thermodynamic Analysis View Full Text


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Article Info

DATE

2013-12

AUTHORS

Vladimir L. Solozhenko, Oleksandr O. Kurakevych

ABSTRACT

Solid-state phase transformations and melting of high-purity crystalline boron have been in situ and ex situ studied at pressures to 20 GPa in the 1500-2500 K temperature range where diffusion processes become fast and lead to formation of thermodynamically stable phases. The equilibrium phase diagram of boron has been constructed based on thermodynamic analysis of experimental and literature data. The high-temperature part of the diagram contains p-T domains of thermodynamic stability of rhombohedral β-B106, orthorhombic γ-B28, pseudo-cubic (tetragonal) t'-B52, and liquid boron (L). The positions of two triple points have been experimentally estimated, i.e. β-t'-L at ~ 8.0 GPa and ~ 2490 K; and β-γ-t' at ~ 9.6 GPa and ~ 2230 K. Finally, the proposed phase diagram explains all thermodynamic aspects of boron allotropy and significantly improves our understanding of the fifth element. More... »

PAGES

2351

References to SciGraph publications

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  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1038/srep02351

    DOI

    http://dx.doi.org/10.1038/srep02351

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1013839331

    PUBMED

    https://www.ncbi.nlm.nih.gov/pubmed/23912523


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